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Data from observations made at the Cape Verde Atmospheric Observatory (CVAO) which exists to advance understanding of climatically significant interactions between the atmosphere and ocean and to provide a regional focal point and long-term data. The observatory is based on Calhau Island of São Vicente, Cape Verde at 16.848N, 24.871W, in the tropical Eastern North Atlantic Ocean, a region which is data poor but plays a key role in atmosphere-ocean interactions of climate-related and biogeochemical parameters including greenhouse gases. It is an open-ocean site that is representative of a region likely to be sensitive to future climate change, and is minimally influenced by local effects and intermittent continental pollution. The dataset contains a longterm record of ozone mixing ratio measurements made from several instruments at the Cape Verde Observatory.